ASTM D6730 DANI Optimized Method without Cryo

Oven

• Initial temperature 35 °C.
• Initial time 15 min.
• First program rate 1 °C/min.
• First hold temperature 60 °C.
• First hold time 20 min.
• Second program rate 2 °C/min.
• Final temperature 200 °C.
• Final hold time 5 min.

Injector

• Temperature 250 °C.
• Split ratio 150:1.
• sample size 0.5 uL.

Detector

• FID.
• Temperature 250 °C.
• Hydrogen 30 mL/min.
• Air 300 mL/min.
• Nitrogen 30 mL/min.

Carrier gas

• Helium, pressure constant: 4.16 bar.