ASTM D6730 DANI Optimized Method with Cryo

Oven

• Initial temperature 5 °C.
• Initial time 10 min.
• First program rate 5 °C/min.
• First hold temperature 50 °C.
• First hold time 0 min.
• Second program rate 1.5 °C/min.
• Final temperature 200 °C.
• Final hold time 5 min.

Injector

• Temperature 250 °C.
• Split ratio 150:1.
• Sample size 0.5 uL

Detector

• FID.
• Temperature 250 °C.
• Hydrogen 30 mL/min.
• Air 300 mL/min.
• Nitrogen 30 mL/min.

Carrier gas

• Helium, pressure constant: 4.16 bar.